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1 H NMR (400 MHz, DMSO- d 6 ) 12.31 (s, 1H), 10.99 (s, 1H), 7.63 (dt, J = 6.6, 3.3 Hz, 1H), 7.597.52 (m, 2H), 7.40 (d, J = 6.9 Hz, 1H), 6.72 (d, J = 3.5 Hz, 1H), 5.13 (dd, J = 13.3, 5.1 Hz, 1H), 4.394.19 (m, 3H), 4.06 (s, 2H), 3.89 (d, J = 13.7 Hz, 1H), 3.09 (t, J = 7.2 Hz, 2H), 3.00 (d, J = 12.5 Hz, 1H), 2.942.86 (m, 1H), 2.73 (t, J = 11.5 Hz, 1H), 2.632.54 (m, 2H), 2.492.42 (m, 1H), 2.322.25 (m, 2H), 2.051.97 (m, 1H), 1.80 (s, 2H), 1.60 (dd, J = 14.3, 7.2 Hz, 2H), 1.46 (ddd, J = 21.9, 14.5, 7.3 Hz, 6H), 1.331.27 (m, 2H), 1.18 (d, J = 4.6 Hz, 9H)

19,20 These dosing ranges (approximately 3x more testosterone undecanoate adjusted for amount as testosterone orally as compared to the buccal dose) are approximately in line with the range we would expect based on the bioavailability information in the literature

Investigations assess cytokine-expression profiles, epithelial-barrier integrity, mucosal architecture, tight-junction organization, and tissue-remodeling responses following experimental enteral delivery