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At the indicated time points after adding formaldehyde (0, 10, 20, 40, 60, 120, 240 and 360 min), a sample was taken and diluted 1:50 in extraction solvent for LCMS measurements (concentration of compounds ~50 M) or 1:10 in water for GCMS-based detection of formaldehyde (highest concentration = 125 M)

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A total of 267 subjects (120 patients and 147 controls) were genotyped for the deletion polymorphism of two GST isoforms

18a, 18b, and 18c, respectively was then washed with DMF (10 times) and ethanol (10 times) and finally dried in vacuo